Growth of NBT template particles through topochemical microcrystal conversion and their structural characterization

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dc.contributor.authorDursun, Sinan
dc.contributor.authorMensur-Alkoy, Ebru
dc.contributor.authorSabuncu, Abdulsamet
dc.contributor.authorBerksoy-Yavuz, Ayse
dc.contributor.authorGulgun, Mehmet Ali
dc.contributor.authorAlkoy, Sedat
dc.date.accessioned2024-07-12T21:51:33Z
dc.date.available2024-07-12T21:51:33Z
dc.date.issued2017en_US
dc.departmentMaltepe Üniversitesien_US
dc.description.abstractIn this study, uniform rectangular plate-like perovskite Na0.5Bi0.5TiO3 templates were obtained by molten salt synthesis method in three steps. Perovskite plate-like Na0.5Bi0.5TiO3 templates were synthesized from bismuth-layered Na0.5Bi4.5Ti4O15 by topochemical microcrystal conversion method at the third and final step. The most important point was that the plate-like morphology remained as desired, but templates were obtained in cubic perovskite structure. The Na2CO3 excess in the third step was the main controlling parameter. The crystalline orientation of the particles was investigated by electron backscatter diffraction analysis. The results indicated that the particles are single crystalline in nature. In the case of the 90mol% excess of the stoichiometric Na2CO3 ratio, the NBT platelets had highly regular, rectangular prismatic morphology and single-crystal nature. The structure was also confirmed through high-resolution transmission electron microscope and selected area electron diffraction analysis.en_US
dc.description.sponsorshipScientific and Technical Research Council of Turkey-TUBITAK [114M518]en_US
dc.description.sponsorshipThis work was financially supported by the Scientific and Technical Research Council of Turkey-TUBITAK through the Project no. 114M518.en_US
dc.identifier.doi10.1111/jace.14653
dc.identifier.endpage944en_US
dc.identifier.issn0002-7820
dc.identifier.issn1551-2916
dc.identifier.issue3en_US
dc.identifier.scopus2-s2.0-85007425306en_US
dc.identifier.scopusqualityQ1en_US
dc.identifier.startpage937en_US
dc.identifier.urihttps://dx.doi.org/10.1111/jace.14653
dc.identifier.urihttps://hdl.handle.net/20.500.12415/8274
dc.identifier.volume100en_US
dc.identifier.wosWOS:000397503100013en_US
dc.identifier.wosqualityQ1en_US
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoenen_US
dc.publisherWILEYen_US
dc.relation.ispartofJOURNAL OF THE AMERICAN CERAMIC SOCIETYen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.snmzKY02055
dc.subjectgrain growthen_US
dc.subjectmolten salt synthesisen_US
dc.subjectNa0.5Bi0.5TiO3 templatesen_US
dc.subjectperovskiteen_US
dc.subjecttopochemical microcrystal conversion (TMC)en_US
dc.titleGrowth of NBT template particles through topochemical microcrystal conversion and their structural characterizationen_US
dc.typeArticle
dspace.entity.typePublication

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